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Research
 

Undergraduate research:Modified Cationic Starch Production by Microwave Technique

  • Advisor: Dr. Wutthichai Nakraksa
  • Partner: Chuleeporn Boonmasiri, Noppamas Nuengthong

Master thesis: Moisture Shelf Life of Packaged Milk Powder

  • Advisor: Dr. Ruben J. Hernandez
  • Related publication/conference

Ph.D dissertation: 1-MCP Controlled Release System to Extend the Shelf Life of Fresh-cut Apples

  • Advisor: Dr. Ruben J. Hernandez, Dr. Bruce Harte
  • Co advisor: Dr. Randolph Beaudry
  • Related publication/conference
    • WorldPak (East Lansing, MI) 2002

Please click here to  see research related documents


Abstract

Modified Cationic Starch Production by Microwave Technique

Study on Cationic starch production by using microwave technique, drying process that can be reduced production time, was done by mixing the tapioca starch with the reagent QUAT188 11.6%(w/v) and NaOH 6.9%(w/v) at the liquid phase:solid phase ratio 0.40:1, 0.50:1 and 0.67:1. The mixture were conditioned at 50C for 8 hrs. The conditioned mixture was ground and sieved pass throught sieve 50 mesh. Then the mixture were heated by using the microwave at the frequency 2450 MHz for 3, 5 and 7 min for cationization reaction. Cationic starch had 2-13% moisture content(%MC), 0.053-0.311% bound nitrogen(%BN) and had the degree of substitution(DS) in the range between 0.006 and 0.037. The reaction efficiency(%RE) was between 6.14 and 36%. The moisture content of the product, the amount of bound nitrogen, the reaction efficiency and the degree of substituion were negative correlation to the heating time and were positive correlation to the ratio between liguid phase and solid phase. The two factors, heating time and liquid phase:solid phase, were effects to %MC of cationic starch 75% and 8%, respectively whlie %BN, DS and %RE 46% and 42-44%, resprctively.


Moisture Shelf Life of Packaged Milk Powder

As new packaging materials become available for non-fat dry milk, there is a need for shelf life simulation to reduce the time and cost needed. In order to perform a simulation, information about product and package characteristics was obtained. GAB equation was employed to describe the moisture sorption isotherm of the product. The barrier properties of packages were described by the permeance of the material since the package is leak proof.

Shelf life simulation consisted of shelf life modeling, model analysis, and model validation. Shelf life modeling was based on mass transfer through the package wall and the GAB equation. From sensitivity analysis of the model, shelf life is most sensitive to the ratio of area to product dry weight and least sensitive to parameter C of GAB equation. Model validation is necessary to ensure the applicability of the model. The shelf life model based on GAB equation is applicable to predict the shelf life of non-fat dry milk packaged in F-flute corrugated board/plastic boxes except for non-fat dry milk package in the poorest barrier package.

 

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